A Perfect Dedome?

A more common name for toluene is toluol.

Its available at Home Hardware in Canada and at Menards in the States. Probably find it at a lot more places if you check.

https://www.menards.com/main/paint/cleaners-thinners-removers/paint-stain-cleaners/thinners-solvents/sunnyside-reg-toluol-1-qt/p-1444444215447.htm

Home Hardware also sells a lacquer thinner made up of toluene, methyl alcohol and methyl ethyl ketone, that seems like a pretty nasty combination.

Mem talked about his method of dedoming being a two step process, attack the glue first then swell the dome off. I can’t figure out if he was using different chemicals or wetting the base of the led for a while and then submerging it.

Thanks, toluol.
Also (under that name) not easy to obtain…

I think it’s banned as a paint thinner in your country. Another name for it is methyl benzene.

Do you recognize any names from this list? http://www.chemspider.com/Chemical-Structure.1108.html

Are there any places around that replace fiberglass boats or kevlar kayaks that you can check with?

Has anyone tried lighter fluid or kerosene yet?

Failing that you can try hot dedoming, this guy makes it look easy. LED reflow & dedome with battery method - YouTube

Well, that wasn’t too difficult afterall.
For the Dutchies:
~~https://www.fixxar.nl/elma-elma-thinner-tolueen-1-l.html~~
Probably not 100% toluene, but i think it’ll do.

(edit) O, dang… Their supplier had it wrong, they sent me normal thinner…
dispute in progress… :weary:

Update: A Perfect Dedome? - #935 by Jerommel

Well , i found here Nitro paint thinner easily , in comparison with ither chemicals that i can’t even order online .

Price was good i think , 3.3€ for 1L .

I think it weakened the bond wires so the led popped …

@Tom I also couldn’t find Nitro thinner. I read somewhere that MEK worked, so I started using it. The SST-40 dedomes nicely with it. The couple of XML2 U4-1A’s I did in it had the usual tint shift.

Readily available at HD. I have only tried it hot, so not sure how well it works cold.

Thanks Scott. Yea, my original plan was to get some MEK, but seems like everyone is only talking about toluene now. I'll get the MEK for now then.

All,

The answer may have been under my nose this whole time (some pun intended there). I’ve been using a solvent called Wil-Bond made by imperial. I don’t recall ever trying to do a full chemical dedome with it for fear of phosphor damage and generally I’m impatient. BUT - I have used it with much success to clean up the bits left behind during my hot dedomes and it seems to make quick work of the silicone scraps. So I looked up the MSDS and compared it to the solvent list I’d linked previously… What I found is that it’s full of theoretically effective solvents. I will say it’s odor is definitely nothing to be taken lightly. Even the can sealed up and in a cupboard, I can smell it on hot days when I walk into my hobby room. The good news is it can be found in the US at Walmart and has free shipping for ~$18

I’ll throw a few sacrificial LEDs in there tonight sometime and see what happens. I don’t think I’ll try heating it at all. Don’t have the appropriate space or heating equipment for that right now.

LEDs that I might have to try…

XP-L
219B
XP-E2
XHP-70
MT-G2 (MAYBE)

I already picked up a quart of MEK on the way home, so may give that a shot this eve.

I got some too! Going to try cold and then hot, in the crock pot!! :smiley:

Just so you know:

:person_facepalming:

Update on previous post:
(only relevant to Dutch dedomers)

It’s a little confusing…
This “ELMA thinner” is sold as ‘thinner-tolueen’ but it doesn’t say ‘tolueen’ anywhere on the bottle, not even in the ‘samenstelling’ (contents).
However, after asking ELMA themselves they assured me there is tolueen in it.
They promised to send me a more detailed list of ingredients.
I will report back on this here.

In Post 74 of the Haikelite HT35 great deal (NOT 49.99) thread, dmsoule wrote:

This sounds promising. Has anyone try lacquer thinner here in the States?

I don't know if lacquer thinner is safer than MEK. I read the Material Safety Data Sheet ("MSDS") for MEK once and it scared me away from the product.

Been testing White Spirit on an old XM-L and newer XM-L2s, a little bath and 3 to 4 days to soften and remove leftovers; does a pretty good job. If in a hurry, bain-marie.

Finally got ahold of straight Toulene!

One BIG problem though… After five minutes in the LED comes off with the dome… Tried it two times with the same results.

Tried one more time and this time without heating the Toluene. It took a long time to get the dome completely clean. But it was totally worth it! For the first time there was not a single hint of green in the tint!

I will post a beamshot later showing this sst-40 against the one done in Nitro thinner.

Here’s a crappy photo taken from my iPhone… Is it even possible to take a good one on the phone?

Left: Sst-40 dedomed in hot Nitro thinner.
Right: Sst-40 dedomed in finger warm Toluene.

Sledgestone, in order for camera pictures be worth comparing chromaticity wise, a common reference point must be used (usually “daylight” or 6500K). If “auto” is used the device will try to detect and compensate the spectra for it to look like daylight, usually with bad results with some sources but good with others (hardware and software dependent too, of course).

The pics look good to me, at least with regards to differentiating the dedoming process turn outs.

I used to soak my LED’s in “wasbenzine”, what translates into: white-spirit; refined petrol; cleaning spirit; cleaning fluid; dry-cleaning naphta. Confused? Not really, the chemical compounds involved are seldom identical from brand to brand. Last time it took 48 hours, and I still managed to tear off the bond wires when removing the residue.
So I ordered some MEK (methyl ethyl keton) and the dome of the SST-40 came off in 2 hours, and much cleaner.